Ultra-Small-Angle X-ray Scattering Facility

X-ray science division, beamline 9ID-C

Mail-in program

Mail-in program

Main-in samples are accepted at the discression of the USAXS staff and can be shipped only after prior agreement of the USAXS staff. Such samples have to satisfy very stringent requirements related to safety and handling... Note, that returning samples to users is quite complicated process (see Instruction for shipping materials from APS for details and review these instructions on what you need to provide). It is usually easier to dispose of the samples at the APS, so please, provide disposal instructions.

Samples must be mounted in one of these below listed two methods:

1. In 25 x 25 x 1.1 (or less) mm sample holders similar ot the Grace bio-lab cells JTR20R and JTR13R. Paper/plastic frames of same dimensions (25 x 25mm) can be made. Thickness can be less than 1mm as long as the frames are sufficently sturdy. These frames must have hole in the center with space for the sample. Maximum hole size can be ~18mm diameter, preferably smaller. Sample needs to be mounted approximately in the center. Minimum sample area available for X-ray beam is 2 x 2 mm. Samples should be supported from sides by tape - use 3M Scotch Magic tape or equivalent, not any other. The 3M Scotch magic tape has very little SAXS signal and is nearly ideal material for sample mounting. If necessary, back the sample with the 3M Scotch Magic tape. In that case send "empty" = sample holder with the tape layers you have used so we can measure it and subtract the tape scattering. For powders, put thin layer of powder on sticky side of this 3M Scotch magic tape and cover with second layer (sticky sides together). This creates little envelope with powder fixed between the tapes. Use powder sparingly, thin layers are required - thick layers of powder samples have multiple scattering! Mount these tape envelopes same as solid samples in frames.

Mark EACH frame with User name, Sample name (less than 15 characters, letters/numbers only). If data should be on absolute intensity scale include sample thickness in millimeters.

2. In Kimbel Chase KIMAX Melting capillaries (or equivalent) - see above for details. Do NOT send thin wall capillaries (Charles Supper), they breake too often in shipping and during sample manipulation at the beamline. Seal end of capillaries by epoxy or other appropriate and reliable method. Fill at least 5 mm of capillary with sample. Attach to the end of capillary sticker with user name and sample name. Sample name must be less than 15 characters (letters/numbers ONLY).

 

Correctly mounted samples (examples):

 

Top: Liquid sample in Grace biol-lab cell with Kapton windows. Alternativelly, you can use also glass for the widnows. Use glass covers slips for microscopy, 25 micron thick, we use Fisherfinest "Premium Cover Glass" Catalog No: 12-548-C, 25x25mm - 1 (mil .. 25micron) from Fisher Scientific. Any similar should work just fine.

 

Center : Grace bio-labs cell mounted powder. Mounted between two 3M Scotch Magic tape layers and then taped over the center of the hole. Include same number of layers of the tape you used to be measured for instrumental curve.

 

Bottom: Carboard paper made holder for solid sample. This sample is held on its side by 3M Scotch magic tape. If the tape is not in the studied area, no need to send if for instrument background measurement.

 

Right: Capillaries. Fill at least 5 mm of capillary with the sample. These are KIMAX melting capillaries, 1.3 - 1.5 mm outside diameter. Seal safely. Attach label with user name and sample name.

INCLUDE capillary for measurement of instrumental curve. Either empty capillary or capillary filled with solvent... Whatever is appropriate for your samples, but we need the correct capillary to measure instrumental background.

Note each sample has user name, sample name and sample thickness on it. Sample thickness is in millimeters.

PRINT and make sure the names can be read easily. Watch handwriting!!! Include in the shippment and e-mail ahead separate list of sample names. Ship according to all valid rules, regulations, and other safety considerations (see shipping).